纳米无定形磷酸钙对渗透树脂显微硬度及抛光性能的影响

doi:10.13701/j.cnki.kqyxyj.2017.06.001

口腔医学研究 ›› 2017, Vol. 33 ›› Issue (6): 581-584.DOI: 10.13701/j.cnki.kqyxyj.2017.06.001

• 名家论道 • 下一篇

纳米无定形磷酸钙对渗透树脂显微硬度及抛光性能的影响

张浩, 孙卫斌, 苗雷英, 葛久禹^*

南京大学医学院附属口腔医院,南京市口腔医院牙体牙髓病科江苏南京 210008)

收稿日期:2016-11-12 出版日期:2017-06-20 发布日期:2017-06-26
通讯作者: 葛久禹,E-mail:JYGe@nju.edu.cn
作者简介:张浩(1989~ ),男,山东人,医师,硕士,主要从事牙体牙髓病临床研究。
基金资助:
国家临床重点专科建设项目经费资助[卫生部卫办医政函(2011)873号]
江苏省科技发展计划项目(BE2011611)

Effects of Amorphous Calcium Phosphate on Microhardness and Polishing Performance of Resin Infiltrant.

ZHANG Hao, SUN Wei-bin, MIAO Lei-ying, Ge Jiu-yu^*.

Nanjing Stomatological Hospital, Medical School of Nanjing University, Nanjing 210008, China.

Received:2016-11-12 Online:2017-06-20 Published:2017-06-26

摘要/Abstract

摘要： 目的:探讨渗透树脂中加入纳米无定形磷酸钙后对树脂显微硬度及抛光性能的影响。方法:通过脱矿液建立人工龋模型,分别使用渗透树脂及加入纳米无定形磷酸钙的渗透树脂对龋模型进行渗透,使用显微硬度测试仪计算努氏硬度,利用扫描电子显微镜观察釉质抛光表面探究无定形磷酸钙加入渗透树脂后对树脂显微硬度及抛光性能的影响。结果:显微硬度测试后发现,渗透树脂组(C组)与脱矿组(B组)相比,显微硬度提高(P<0.05),但较正常釉质组(A组),硬度值存在统计学差异(P<0.05),纳米无定型磷酸钙渗透树脂组(D组)与正常釉质组(A组)相比,无统计学差异。扫描电镜观察显示,渗透树脂组(C组)及纳米无定形磷酸钙渗透树脂组(D组)经过相同步骤的抛光后,渗透树脂组(C组)表面光滑,孔隙小而少,有少量细滑痕,纳米无定形磷酸钙渗透树脂组(D组)表面不规整,孔隙较大,较C组显粗糙。结论:渗透树脂虽然可以较好恢复脱矿釉质表面的显微硬度,但与正常釉质存在差异,纳米无定形磷酸钙的加入,可以较好弥补渗透树脂这一缺点,但是会影响树脂的抛光性能。

关键词: 无定形磷酸钙, 渗透树脂, 显微硬度, 抛光性能

Abstract: Objective: To investigate the effects of amorphous calcium phosphate on microhardness and polishing performance of resin infiltrant. Methods: Artificial model of dentin caries lesion was established by demineralization fluid treating on the enamel. The specimens were infiltrated by resin infiltrant or resin infiltration mixed with amorphous calcium phosphate agent. Microhardness was investigated by the microhardness tester and the polishing performance was investigated by scanning electron microscopy. Results: The microhardness of resin infiltration group was higher than that of demineralized group (P<0.05), but lower than that of normal enamel group (P<0.05). There were no statistical differences between the nano amorphous calcium phosphate group and the normal enamel group. In the resin infiltration group, the enamel was smoother with smaller amount of slide mark and smaller pores on the surface in resin infiltration group observed by scanning electron microscope. The surface was rougher with big pores in the nano amorphous calcium phosphate group. Conclusion: Resin infiltration can improve the microhardness of demineralized enamel surface. The nano amorphous calcium phosphate mixed with the resin infiltration can improve the microhardness but decrease the polishing performance.

Key words: Amorphous calcium phosphate , Resin infiltration, Microhardness, Polishing performance

中图分类号:

R780.1

张浩, 孙卫斌, 苗雷英, 葛久禹. 纳米无定形磷酸钙对渗透树脂显微硬度及抛光性能的影响[J]. 口腔医学研究, 2017, 33(6): 581-584.

ZHANG Hao, SUN Wei-bin, MIAO Lei-ying, Ge Jiu-yu.. Effects of Amorphous Calcium Phosphate on Microhardness and Polishing Performance of Resin Infiltrant.[J]. Journal of Oral Science Research, 2017, 33(6): 581-584.

参考文献

[1] Mahoney E, Holt A, Swain M, et al. The hardness and modulus of elasticity of primary molar teeth: an ultra-micro-indentation study [J]. J Dent, 2000, 28(8)∶589-594
[2] Santos MJMC, Passos SP. Hardening of a dual-cure resin cement using QTH and LED curing units [J]. J Appl Oral Sci, 2010, 18(2)∶110-115
[3] Adebayo OA, Burrow MF, Tyas MJ. Enamel microhardness and bond strengths of self-etching primer adhesives [J]. Eur J Oral Sci, 2010, 118(2)∶191-196
[4] Fennis WMM, Ray NJ, Creugers NHJ. Microhardness of resin composite materials light-cured through fiber reinforced composite [J]. Dent Mater, 2009, 25(8)∶947-951
[5] 徐辉,周新文,华幸,等.渗透树脂对正畸后脱矿牙釉质表面显微硬度的影响[J].口腔医学研究,2013,29(3)∶252-254
[6] 赵晓一,高学军.渗透树脂治疗对人工釉质龋表面微硬度影响的研究[J].牙体牙髓牙周病学杂志,2014,24(8)∶455-459
[7] Paris S, Meyer-Lueckel H, Coelfen H, et al. Resin infiltration of artificial enamel caries lesions with experimental light curing resins [J]. Dent Mater J, 2007, 26(4)∶582-588
[8] Paris S, Schwendicke F, Seddig S, et al. Micro-hardness and mineral loss of enamel lesions after infiltration with various resins: influence of infiltrant composition and application frequency in vitro [J]. J Dent,2013,41(6)∶543-548
[9] Asmussen E, Peutzfeldt A. Influence of UEDMA, BisGMA and TEGDMA on selected mechanical properties of experimental resin composites [J]. Dent Mater, 1998, 14(1)∶51-56
[10] Sergey V. Dorozhkin. Amorphous calcium (ortho) phosphates [J]. Acta Biomaterialia, 2010, 6(12)∶4457-4475
[11] Wilder EA,Wilson KS,Quinn JB.Effect of an organogelator on the properties of dental composites [J]. Chem Mater,2005,17(11)∶2946-2952
[12] Xu HH, Moreau JL, Sun L, et al. Nanocomposite containing amorphous calcium phosphate nanoparticles for caries inhibition [J]. Dent Mater, 2011, 27(8)∶762-769
[13] Hefferren JJ, Koehler HM. Foods, nutrition and dental health [M],1981∶138
[14] Skrtic D, Antonucci JM, Eanes ED. Improved properties of amorphous calcium phosphate fillers in remineralizing resin composites [J]. Dent Mater, 1996, 12(5)∶295-301
[15] W.F.Regnault,T.B.Icenogle,J.M.Antonucci, et al. Amorphous calcium phosphate/urethane methacrylate resin composites. I. Physicochemical characterization [J]. J Mater Sci Mater Med, 2008, 19(2)∶507-515
[16] Antonucci JM, Skrtic D. Matrix resin effects on selected physicochemical properties of amorphous calcium phosphate composites [J]. J Bioact Comp Polym, 2005, 20(1)∶29-49
[17] 张浩,苗雷英,葛久禹,等.无定形磷酸钙对渗透树脂颜色稳定性及渗透性影响研究[J].中国实用口腔科杂志,2015,8(3)∶158-161
[18] Lee SY, Regnault WF, Antonucci JM, et al. Effect of particle size of an amorphous calcium phosphate filler on the mechanical strength and ion release of polymeric composites [J]. J Biomed Mater Res B Appl Biomater,2007,80(1)∶11-17
[19] Skrtic D, Hailer AW, Takagi S, Antonucci JM, Eanes ED. Quantitative assessment of the efficacy of amorphous calcium phosphate/methacrylate composites in remineralizing caries-like lesions artificially produced in bovine ename [J]. J Dent Res,1996,75(9)∶1679-1686
[20] O’Brien WJ. Dental materials and their selection [M]. 3rd ed.Berlin: Quintessence Publishing,2002
[21] Venturini D, Cenci MS, Demarco FF, et al. Effect of polishing techniques and time on surface roughness. Hardness and microleakage of resin composite restorations [J]. Oper Dent, 2006,31(1)∶11-17

纳米无定形磷酸钙对渗透树脂显微硬度及抛光性能的影响

Effects of Amorphous Calcium Phosphate on Microhardness and Polishing Performance of Resin Infiltrant.

PDF (PC)

可视化

被引次数

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 9

编辑推荐

Metrics

[1]	王金凤, 车静怡, 刘会梅, 朱兴国, 孙文章, 潘爽. 黄瓜籽醇提取物对早期釉质龋再矿化的影响[J]. 口腔医学研究, 2020, 36(1): 65-69.
[2]	徐泽先, 杨彦伟, 邱宜农, 李志强, 王学锋, 王锐, 郑欣, 刘斌. 核壳状CHX/ACP纳米球改性流体树脂的体外释药研究[J]. 口腔医学研究, 2019, 35(9): 898-901.
[3]	代建梅, 李奉华, 邱喜丽, 董新. 渗透树脂和生物活性玻璃修复早期釉质龋的研究[J]. 口腔医学研究, 2019, 35(5): 453-456.
[4]	张浩, 孙卫斌, 苗雷英, 葛久禹. 不同渗透性材料对早期釉质龋渗透性能影响的研究[J]. 口腔医学研究, 2019, 35(4): 328-330.
[5]	宋金花, 刘宗仁, 刘文超, 张旭, 李彦秋. 羧甲基壳聚糖-溶菌酶纳米凝胶稳定无定形磷酸钙促进脱矿牙釉质再矿化[J]. 口腔医学研究, 2018, 34(8): 828-831.
[6]	孟庆飞，张甲第，孟箭. Opalescence皓齿美白联合ICON渗透树脂治疗氟斑牙的疗效观察[J]. 口腔医学研究, 2017, 33(9): 987-990.
[7]	梁向阳,孔晶晶,李春年,李安. 不同材料在碳酸饮料所致脱矿釉质再矿化中的作用[J]. 口腔医学研究, 2017, 33(12): 1274-1277.
[8]	邢文忠,蒋滔,李蓉,梁珊珊,王贻宁. 家庭漂白剂对复合树脂表面粗糙度、显微硬度的影响[J]. 口腔医学研究, 2015, 31(9): 871-875.
[9]	钟洁,林碧琛,陈小贤. 渗透树脂对青少年前牙白垩斑龋损治疗效果的初步研究[J]. 口腔医学研究, 2015, 31(2): 163-166.