微量Ti-6Al-4V掺杂对SLM打印纯钛机械性能与显微结构的影响

doi:10.13701/j.cnki.kqyxyj.2024.08.006

口腔医学研究 ›› 2024, Vol. 40 ›› Issue (8): 693-699.DOI: 10.13701/j.cnki.kqyxyj.2024.08.006

微量Ti-6Al-4V掺杂对SLM打印纯钛机械性能与显微结构的影响

阿伊森·赛米, 何俊杰, 张文娜, 骆小平^*

南京大学医学院附属口腔医院,南京市口腔医院,南京大学口腔医学研究所江苏南京 210001

收稿日期:2024-01-10 出版日期:2024-08-28 发布日期:2024-08-22
通讯作者: *骆小平,E-mail:l_xiaoping@yahoo.com
作者简介:阿伊森·赛米(1993~ ),女,乌鲁木齐人,硕士,医师,主要从事增材制造材料与临床修复体相关研究。
基金资助:
江苏省科技厅重点研发计划(编号:BE2021608)

Mechanical Properties and Microstructure of Pure Titanium through Adding Trace Ti-6Al-4V Powder in SLM Manufacturing

SAIMI·Ayisen, HE Junjie, ZHANG Wenna, LUO Xiaoping^*

Nanjing Stomatological Hospital, Affiliated Hospital of Medical School, Nanjing University, Nanjing 210001, China

Received:2024-01-10 Online:2024-08-28 Published:2024-08-22

摘要/Abstract

摘要： 目的: 探究选区激光熔化(selective laser melting,SLM)打印制造的添加微量Ti-6Al-4V粉末的纯钛材料,在两种不同热处理温度(650 ℃,2 h和700 ℃,2 h)及不同扫描速度(1000 mm/s和500 mm/s)下的机械性能。方法: 制备SLM打印的试样,测试材料的机械性能,观察拉伸试样的断口形貌及显微结构。结果: SLM打印的纯钛试样的极限拉伸强度在1000 mm/s扫描速度时高于500 mm/s扫描速度时的25%;在650 ℃及700 ℃不同热处理条件下,650 ℃,2 h在两种扫描速度下都表现出更加优异的机械性能,但延伸率在700 ℃,2 h在低扫描速度组更高。结论: 添加微量Ti-6Al-4V粉末后打印的纯钛材料相较于Ti-6Al-4V合金更能满足口腔修复体的要求。

关键词: 选区激光熔化, 增材制造, 义齿支架, 机械性能, 钛, Ti-6Al-4V, 合金, 热处理

Abstract: Objective: To investigate the mechanical properties of pure titanium by adding trace Ti-6Al-4V powder in SLM printing manufacturing at two different heat treatment temperatures (650 ℃,2 h and 700 ℃,2 h) and different scanning speeds (1000 mm/s and 500 mm/s). Methods: SLM samples with two different scanning speed (GA:1000 mm/s,GB:500 mm/s) were prepared and heat treated with 650 ℃,2 h (HT1) and 700 ℃,2 h (HT2). The mechanical properties of the materials were tested, and the fracture morphology and microstructure were observed with LSCM and SEM. Results: The tensile strength of SLM printed pure titanium samples was higher at 1000 mm/s(>20%), and the elongation was higher at 500 mm/s. Consistent annealing revealed that the 650 ℃, 2 h treatment yielded outstanding mechanical performance at both scanning speeds. Conclusion: SLM-ed pure titanium material by adding trace Ti-6Al-4V powder can better meet the requirements of oral restorations compared to SLM-ed Ti-6Al-4V alloy.

Key words: selective laser melting, additive manufacturing, denture framework, mechanical properties, titanium, Ti-6Al-4V, alloy, heat treatment

阿伊森·赛米, 何俊杰, 张文娜, 骆小平. 微量Ti-6Al-4V掺杂对SLM打印纯钛机械性能与显微结构的影响[J]. 口腔医学研究, 2024, 40(8): 693-699.

SAIMI·Ayisen, HE Junjie, ZHANG Wenna, LUO Xiaoping. Mechanical Properties and Microstructure of Pure Titanium through Adding Trace Ti-6Al-4V Powder in SLM Manufacturing[J]. Journal of Oral Science Research, 2024, 40(8): 693-699.

参考文献

[1] Wang Z, Tan Y, Li N. Powder metallurgy of titanium alloys: A brief review [J]. J Alloys Compd, 2023: 965.
[2] Eujin Pei AB, Dongdong Gu,Christoph Klahn. Handbook of Additive Manufacturing[M]. Switzerland: Springer. 2023.
[3] Korkmaz ME, Gupta MK, Waqar S, et al. A short review on thermal treatments of Titanium & Nickel based alloys processed by selective laser melting [J]. J Mater Res, 2022, 16: 1090-1101.
[4] Takaichi A, Fueki K, Murakami N, et al. A systematic review of digital removable partial dentures. Part Ⅱ: CAD/CAM framework, artificial teeth, and denture base [J]. J Prosthodont Res, 2022, 66(1): 53-67.
[5] Peng PW, Hsu CY, Huang HY, et al. Trueness of removable partial denture frameworks additively manufactured with selective laser melting [J]. J Prosthet Dent, 2022, 127(1): 122-127.
[6] Tshephe TS, Akinwamide SO, Olevsky E, et al. Additive manufacturing of titanium-based alloys- A review of methods, properties, challenges, and prospects [J]. Heliyon, 2022, 8(3): e09041.
[7] Hoque ME, Showva NN, Ahmed M, et al. Titanium and titanium alloys in dentistry:current trends ,recent developments, and future prospectes [J]. Heliyon, 2022, 8(11):e11300.
[8] Petrini M, Mangano C, Cellini L, et al. Material characterization and bacterial interaction of titanium discs produced by selective laser melting [J]. Mater Charact, 2022, 189:111989.
[9] Poli PP, de Miranda FV, Polo TOB, et al. Titanium Allergy Caused by Dental Implants: A Systematic Literature Review and Case Report [J]. Materials (Basel), 2021, 14(18):5239.
[10] Fischer RD, Harvill GC, Zhao R, et al. A roadmap for tailoring the microstructure and mechanical properties of additively manufactured commercially-pure titanium [J]. Mater Sci Eng, A, 2024, 892:146088.1-146088.11.
[11] Popovich A, Sufiiarov V, Borisov E, et al. Microstructure and mechanical properties of Ti-6Al-4V manufactured by SLM [J]. Key Eng Mater, 2015, 651-653: 677-682.
[12] Khorasani AM, Gibson I, Ghaderi A, et al. Investigation on the effect of heat treatment and process parameters on the tensile behaviour of SLM Ti-6Al-4V parts [J]. Int J Adv Manuf Technol, 2018, 101(9-12): 3183-3197.
[13] Zhao ZY, Li L, Bai PK, et al. The heat treatment influence on the microstructure and hardness of TC4 titanium alloy manufactured via selective laser melting [J]. Materials (Basel), 2018, 11(8):1318.
[14] Sun D, Gu D, Lin K, et al. Selective laser melting of titanium parts: Influence of laser process parameters on macro- and microstructures and tensile property [J]. Powder Technol, 2019, 342: 371-379.
[15] Vilaro T, Colin C, Bartout JD. As-fabricated and heat-treated microstructures of the Ti-6Al-4V alloy processed by selective laser melting [J]. Metall Mater Trans A, 2011, 42(10): 3190-3199.
[16] Li CL, Wang CS, Narayana PL, et al. Formation of equiaxed grains in selective laser melted pure titanium during annealing [J]. J Mater Res Technol, 2021, 11: 301-311.
[17] 胡丹丹,任灿霞,骆小平.表面处理对激光选区熔化成型纯钛钛瓷结合强度的影响[J].上海口腔医学,2023,32(3):230-235.
[18] 任灿霞,胡丹丹,阿伊森·赛米,等.激光选区熔化成型纯钛不同表面处理对钛-聚合瓷结合强度的研究[J].口腔医学研究,2023,39(5):429-434.
[19] 黄罡骆,庞恩林,孟翔峰,等.激光选区熔化技术制作纯钛可摘义齿支架的可行性研究[J].中国实用口腔科杂志,2020,13(1): 25-29.
[20] Cordeiro JM, Barao VAR. Is there scientific evidence favoring the substitution of commercially pure titanium with titanium alloys for the manufacture of dental implants? [J]. Mater Sci Eng C Mater Biol Appl, 2017, 71: 1201-1215.
[21] Luo M, Lin T, Zhou L, et al. Deformation behavior and tensile properties of the semi-equiaxed microstructure in near alpha titanium alloy [J]. Materials (Basel), 2021, 14(12):3380.
[22] Bajunaid SO, Altwaim B, Alhassan M, et al. The fit accuracy of removable partial denture metal frameworks using conventional and 3D printed techniques: An in vitro study [J]. J Contemp Dent Pract, 2019, 20(4):476-481.
[23] Singh SN, Chowdhury S, Nirsanametla Y, et al. A comparative analysis of laser additive manufacturing of high layer thickness pure Ti and inconel 718 alloy materials using finite element method [J]. Materials (Basel), 2021, 14(4):876.
[24] Li H, Ramezani M, Chen Z, et al. Effects of process parameters on temperature and stress distributions during selective laser melting of Ti-6Al-4V [J]. Trans Indian Inst Met, 2019, 72(12): 3201-3214.
[25] 高明香,王建宏,任杰,等. 扫描策略对选区激光熔化钴铬合金组织和性能的影响[J].激光杂志,2020,41(1): 133-136.
[26] 张志雄,王涛,林鹏,等. 钛合金多向锻造工艺研究进展[J].塑性工程学报,2020,27(8): 1-9.
[27] Dong Y, Li Y, Ebel T, et al. Cost-affordable, high-performance Ti-TiB composite for selective laser melting additive manufacturing [J]. J Mater Res, 2020, 35(15): 1922-1935.
[28] Shen LC, Yang XH, Ho JR, et al. Effects of build direction on the mechanical properties of a martensitic stainless steel fabricated by selective laser melting [J]. Materials (Basel), 2020, 13(22):5142.

微量Ti-6Al-4V掺杂对SLM打印纯钛机械性能与显微结构的影响

Mechanical Properties and Microstructure of Pure Titanium through Adding Trace Ti-6Al-4V Powder in SLM Manufacturing

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