Influence of Pre-phosphoric Acid Etching on Bonding Strength of Two-step Self-etching Adhesives to Enamel

doi:10.13701/j.cnki.kqyxyj.2019.08.007

Abstract

Abstract: Objective: To investigate the effects of phosphoric acid (P) etching pretreatment on the bonding strength of two-step self-etching adhesives SE BOND (SE) and VERSA (VE) to enamel. Methods: 18 fresh and intact bovine incisors were selected and divided into 6 groups according to using pre-phosphoric acid etching and primer (solution ①) or not: SE①+SE②; P+SE①+SE②; P+SE②; VE①+VE②; P+VE①+VE②; P+VE②. The micro-tensile bond strength (MPa) was measured. The enamel samples treated with phosphoric acid, SE① solution, phosphoric acid + SE① solution, VE① solution, and phosphoric acid + VE① solution were observed with SEM. Results: The difference of the microtensile bond strengths of SE①+SE②, P+SE①+SE②, and P+SE② was not statistically significant (P>0.05). The microtensile bond strengths of the P+VE①+VE② group was significantly higher than the VE①+VE② group (P<0.05). The SEM presented a typical honeycomb structure of enamel surface after phosphoric acid treatment. However, SE① solution and VE① solution did not change the enamel surface obviously, which was covered by the smear layer. Conclusion: Phosphoric acid pretreatment improves the microtensile bond strength of VE to enamel. When phosphoric acid pretreatment was applied on enamel surface, primer (solution ①) still be recommended.

Key words: two-step self-etching adhesive, enamel, bond strength, phosphoric acid

LI Xiuhua, YU Peng, TIAN Fucong, WANG Xiaoyan. Influence of Pre-phosphoric Acid Etching on Bonding Strength of Two-step Self-etching Adhesives to Enamel[J]. Journal of Oral Science Research, 2019, 35(8): 748-751.

References

[1] Delbons FB, Perdigão J, Araujo E, et al. Randomized clinical trial of four adhesion strategies in posterior restorations-18-month results[J]. J Esthet Restor Dent, 2015, 27(2): 107-117.
[2] Wellington L, Evandro P, Adriana F. Bond strength of universal adhesives: A systematic review and meta-analysis [J]. J Dent, 2015, 43(7): 765-776.
[3] Kiremitçi A, Yalçin F, Gökalp S. Bonding to enamel and dentin using self-etching adhesive systems [J]. Quintessence Int, 2004, 35(5):367-370.
[4] Erhardt MC, Cavalcante LM, Pimenta LA. Influence of phos-phoric acid pretreatment on self-etching bond strengths [J]. J Esthet Restor Dent, 2004, 16(1):33-41.
[5] Ricardo W, Edward J, Lee W, et al. Enamel and dentin bond strengths of a new self-etch adhesive system [J]. J Esthet Restor Dent, 2011, 23(6): 390-396.
[6] Norbert K, David T, Susanne L, et al. Status of ten self-etch adhesives for bonding to dentin of primary teeth [J]. Int J Paediatr Dent, 2014, 24(3):192-199.
[7] Takaaki S, Tomohiro T, Naoko M, et al. Morphological evaluation of the adhesive/enamel interfaces of two-step self-etching adhesives and multimode one-bottle self-etching adhesives [J]. J Adhes Dent, 2016, 18(3): 223-229.
[8] David HP, Franklin RT, Lorenzo B, et al. State of the art etch-and-rinse adhesives [J]. Dent Mater, 2011, 27(1) :1-34.
[9] Toshiki T, Wayne WB, Akimasa T, et al. Influence of pre-etching times on fatigue strength of self-etch adhesives to enamel [J]. J Adhes Dent, 2016, 18(6): 501-511.
[10] 吕林虎,周会,黎佳灵,等.磷酸浓度对氟斑牙牙釉质微拉伸粘接强度影响的研究[J].口腔医学研究,2017,33(1):51-54.
[11] Weerasinghe DS, Nikaido T, Wettasinghe KA, et al. Micro-shear bond strength and morphological analysis of a self-etching primer adhesive system to fluorosed enamel [J]. J Dent, 2005, 33(5):419-426.
[12] Kumiko Y, Noriyuki N, Satoshi H, et al. Chemical interaction of glycero-phosphate dimethacrylate (GPDM) with hydroxyapatite and dentin [J]. Dent Mater, 2018, 34(7): 1072-1081.
[13] Toshiki T, Wayne WB, Akimasa T, et al. Effect of phosphoric acid pre- etching on fatigue limits of self- etching adhesives [J]. Oper Dent, 2015, 40(3): 379-396.
[14] Peumans M, De Munck J, Van Landuyt K,et al. Thirteen-year randomized controlled clinical trial of a two-step self-etch adhesive in non-carious cervical lesions [J]. Dent Mater, 2015, 31(3): 308-314.

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